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- W4297177522 abstract "The first total synthesis of vanilloloside, calleryanin, and a series of naturally occurring ω-esters of vanilloloside was realized through direct glycosylation of vanillin-based aglycones or late-stage derivatization of vanilloloside. All aglycones and their fragments were synthesized from vanillin as the sole aromatic precursor. Subsequently, these intermediates were used to construct various vanillin-derived glucoside ω-esters using a mild acidic deacetylation as the key synthetic step, providing the final products in the total yields of 10–50% and general purity of >95%. Additionally, the first operationally simple and sustainable synthesis of litseafoloside B was realized on large scale, avoiding the use of toxic solvents and reagents, providing an attractive alternative to isolation of this and other similar compounds from plant sources." @default.
- W4297177522 created "2022-09-27" @default.
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- W4297177522 date "2022-12-01" @default.
- W4297177522 modified "2023-10-03" @default.
- W4297177522 title "Scalable total synthesis of natural vanillin-derived glucoside ω-esters" @default.
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- W4297177522 doi "https://doi.org/10.1016/j.carres.2022.108683" @default.
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