FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W4298149647> ?p ?o ?g. }

• W4298149647 endingPage "340452" @default.
• W4298149647 startingPage "340452" @default.
• W4298149647 abstract "We developed a fast, selective, and sensitive method for the determination of various neutral and acidic phytocannabinoids with an emphasis on the separation of structurally related compounds. Optimized ultra-high performance supercritical fluid chromatography (UHPSFC) allowed the separation of 2 groups of structural isomers, including isomers of m/z 357: cannabidiolic and Δ9-tetrahydrocannabinolic acid, and isomers of m/z 315: cannabichromene, Δ9-tetrahydrocannabinol, Δ8-tetrahydrocannabinol, cannabicyclol, and cannabidiol only in mere 3.5 min followed by 1.5 min equlibration. The 2-ethylpyridine functionalized stationary phase and gradient elution using mobile phase comprising carbon dioxide and methanol: acetonitrile (25:75) + 5% water mixture were selected after the optimization. Tandem mass spectrometry (MS/MS) with electrospray ionization in positive and negative modes with methanol + 5% water as a make-up solvent provided adequate selectivity and sensitivity needed for analysis of phytocannabinoids in complex matrices. The limits of quantification were in the range 0.01-0.5 ng/mL for most of the monitored cannabinoids. The optimized UHPSFC-MS/MS method was then used for the determination of cannabinoids in various products, such as dietary supplements, nutraceuticals, and cosmetics. Solvent extraction methods were optimized for the cosmetic and nutraceutical products with the accuracy in the range 80.4-120.6% and precision 0.5-18.9%. To extract cannabinoids from the herbal infusion matrix, supercritical fluid extraction (SFE) and pressurized liquid extraction (PLE) methods were developed using environmentally friendly solvents water, ethanol, and carbon dioxide. The detailed optimization of extraction solvent composition, temperature, and pressure was carried out with the emphasis on avoiding the thermal degradation of cannabinoids. Optimized SFE and PLE methods were compared and applied to different herbal infusions to confirm declared cannabinoids content." @default.
• W4298149647 created "2022-10-01" @default.
• W4298149647 creator A5010710735 @default.
• W4298149647 creator A5023026842 @default.
• W4298149647 creator A5037800103 @default.
• W4298149647 creator A5038193861 @default.
• W4298149647 date "2022-11-01" @default.
• W4298149647 modified "2023-09-28" @default.
• W4298149647 title "Supercritical fluids in analysis of cannabinoids in various Cannabis products" @default.
• W4298149647 cites W1579321490 @default.
• W4298149647 cites W1918952402 @default.
• W4298149647 cites W1960007621 @default.
• W4298149647 cites W2012678037 @default.
• W4298149647 cites W2014249895 @default.
• W4298149647 cites W2048111489 @default.
• W4298149647 cites W2061737468 @default.
• W4298149647 cites W2073052279 @default.
• W4298149647 cites W2074307018 @default.
• W4298149647 cites W2076545826 @default.
• W4298149647 cites W2082466552 @default.
• W4298149647 cites W2119460233 @default.
• W4298149647 cites W2120227293 @default.
• W4298149647 cites W2135015648 @default.
• W4298149647 cites W2155449454 @default.
• W4298149647 cites W2158197340 @default.
• W4298149647 cites W2187274362 @default.
• W4298149647 cites W2404466761 @default.
• W4298149647 cites W2531214067 @default.
• W4298149647 cites W2562656310 @default.
• W4298149647 cites W2592373681 @default.
• W4298149647 cites W2596854544 @default.
• W4298149647 cites W2605002573 @default.
• W4298149647 cites W2620956212 @default.
• W4298149647 cites W2754568794 @default.
• W4298149647 cites W2762303831 @default.
• W4298149647 cites W2766412939 @default.
• W4298149647 cites W2775640882 @default.
• W4298149647 cites W2793181068 @default.
• W4298149647 cites W2794580413 @default.
• W4298149647 cites W2805120324 @default.
• W4298149647 cites W2888159618 @default.
• W4298149647 cites W2890071983 @default.
• W4298149647 cites W2894853360 @default.
• W4298149647 cites W2901597697 @default.
• W4298149647 cites W2901627119 @default.
• W4298149647 cites W2906793873 @default.
• W4298149647 cites W2912245489 @default.
• W4298149647 cites W2914223045 @default.
• W4298149647 cites W2917121152 @default.
• W4298149647 cites W2924068868 @default.
• W4298149647 cites W2925702123 @default.
• W4298149647 cites W2956964146 @default.
• W4298149647 cites W2970675686 @default.
• W4298149647 cites W2995265395 @default.
• W4298149647 cites W2998721673 @default.
• W4298149647 cites W2999367331 @default.
• W4298149647 cites W3015174780 @default.
• W4298149647 cites W3020580331 @default.
• W4298149647 cites W3033800832 @default.
• W4298149647 cites W3035028232 @default.
• W4298149647 cites W3126002431 @default.
• W4298149647 cites W3164160477 @default.
• W4298149647 cites W3192512174 @default.
• W4298149647 cites W3199949604 @default.
• W4298149647 cites W3201419180 @default.
• W4298149647 cites W3213861470 @default.
• W4298149647 doi "https://doi.org/10.1016/j.aca.2022.340452" @default.
• W4298149647 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36257737" @default.
• W4298149647 hasPublicationYear "2022" @default.
• W4298149647 type Work @default.
• W4298149647 citedByCount "1" @default.
• W4298149647 countsByYear W42981496472023 @default.
• W4298149647 crossrefType "journal-article" @default.
• W4298149647 hasAuthorship W4298149647A5010710735 @default.
• W4298149647 hasAuthorship W4298149647A5023026842 @default.
• W4298149647 hasAuthorship W4298149647A5037800103 @default.
• W4298149647 hasAuthorship W4298149647A5038193861 @default.
• W4298149647 hasConcept C118419359 @default.
• W4298149647 hasConcept C134458231 @default.
• W4298149647 hasConcept C162356407 @default.
• W4298149647 hasConcept C178790620 @default.
• W4298149647 hasConcept C179998833 @default.
• W4298149647 hasConcept C185592680 @default.
• W4298149647 hasConcept C199919908 @default.
• W4298149647 hasConcept C203147553 @default.
• W4298149647 hasConcept C2779607525 @default.
• W4298149647 hasConcept C2780471494 @default.
• W4298149647 hasConcept C40684141 @default.
• W4298149647 hasConcept C43617362 @default.
• W4298149647 hasConcept C4725764 @default.
• W4298149647 hasConceptScore W4298149647C118419359 @default.
• W4298149647 hasConceptScore W4298149647C134458231 @default.
• W4298149647 hasConceptScore W4298149647C162356407 @default.
• W4298149647 hasConceptScore W4298149647C178790620 @default.
• W4298149647 hasConceptScore W4298149647C179998833 @default.
• W4298149647 hasConceptScore W4298149647C185592680 @default.
• W4298149647 hasConceptScore W4298149647C199919908 @default.
• W4298149647 hasConceptScore W4298149647C203147553 @default.

• next