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- W4300506585 abstract "Electro-deoxidation reduction technology is a very attractive method used to treat oxides in metallurgical industry. In this paper, cyclic voltammetry, square wave voltammetry and open circuit chronopotentiometry were applied to study the electrochemical behavior of MoO 3 cathode in the CaCl 2 -NaCl melt at 873 K. Through the electrolytic reduction of MoO 3 at different potentials (−1.15 V, −1.45 V and −1.75 V, vs Ag/AgCl) and XRD analysis, MoO 3 was found to be transformed into several intermediate compounds (CaMoO 4 , MoO 2 and Na 1.4 Mo 2 O 4 ) and finally reduced to metallic Mo. When the electrolysis time was increased from 3 to 18.5 h and the employed potential was reduced from −1.75 V to −2.30 V (vs Ag/AgCl), the intermediate compounds could be completely reduced to metallic Mo, and the reduction ratio of MoO 3 was calculated to be 93.7%." @default.
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- W4300506585 date "2022-08-01" @default.
- W4300506585 modified "2023-09-30" @default.
- W4300506585 title "The Electrolytic Reduction of MoO<sub>3</sub> in CaCl<sub>2</sub>-NaCl Molten Salt" @default.
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- W4300506585 doi "https://doi.org/10.1149/1945-7111/ac87d2" @default.
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