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- W4300961489 abstract "• Isolation of the metal azolate/carboxylate frameworks [Co 3 (HPZTC) 2 (H 2 O) 6 ]·2H 2 O (MAC-1), [Co(H 2 PZTC)(DMF)(H 2 O)] 2 (MAC-2) and [Cd 2 (PZTC)(H 2 O) 2 ] (MAC-3) • MAC-1 features 1-D chains alternating monomeric and dimeric units. • MAC-2 contains 1-D hydrogen-bonded strands of dimeric units. • MAC-3 shows a 3-D non-porous network. The tetratopic ligand 1- H -pyrazol-3,4,5-tricarboxylic acid (H 4 PZTC) has been used for the first time to prepare the new metal azolate/carboxylate (MAC) frameworks [Co 3 (HPZTC) 2 (H 2 O) 6 ]·2H 2 O ( MAC-1 ), [Co(H 2 PZTC)(DMF)(H 2 O)] 2 ( MAC-2 ) and [Cd 2 (PZTC)(H 2 O) 2 ] ( MAC-3 ), along either conventional or solvothermal routes. As assessed by thermogravimetric analysis, before decomposition the three MAC frameworks undergo partial decarboxylation over 200 °C. Powder X-ray diffraction unveiled 1-D chains alternating monomeric and dimeric units in MAC-1 , 1-D hydrogen bonded strands of dimeric units in MAC-2 and a 3-D non-porous network in MAC-3 ." @default.
- W4300961489 created "2022-10-04" @default.
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- W4300961489 date "2023-01-01" @default.
- W4300961489 modified "2023-10-15" @default.
- W4300961489 title "Synthesis and structural characterization of metal azolate/carboxylate frameworks incorporating the 1-H-pyrazol-3,4,5-tricarboxylate ligand" @default.
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- W4300961489 doi "https://doi.org/10.1016/j.ica.2022.121236" @default.
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