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- W4301202222 abstract "Nanocomposites of partially exfoliated structures, based on poly(ethyl methacrylate) (PEMA) were successfully prepared in dioxan at room temperature via in situ polymerization initiated by a Ni(II)α-benzoinoxime complex in presence of 1.5 by weight of an organically modified Algerian bentonite (OBT). Increasing OBT loading from 1.5 to 3% led to nanocomposites of mixed intercalated/exfoliated structures with randomly dispersed OBT stacks, of thickness varying between 17 and 34 nm. The structure of these nanocomposites was investigated by X-ray diffraction and transmission electron microscopy. The glass transition temperature of these nanocomposites increased by 4 °C compared to that of PEMA. Moreover, a thermogravimetry analysis confirmed a significant enhanced thermal stability of PEMA/OBT nanocomposites compared to virgin PEMA prepared under the same conditions. The apparent activation energies Eα of thermal degradation for PEMA/OBT nanocomposites, estimated using Tang's method were much higher than that of virgin PEMA and depended on OBT loading." @default.
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- W4301202222 date "2013-03-01" @default.
- W4301202222 modified "2023-10-18" @default.
- W4301202222 title "Elaboration and thermal behavior of nanocomposites based on poly(ethyl methacrylate) and an Algerian bentonite prepared via in situ polymerization initiated by Ni(II)α-benzoinoxime complex" @default.
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- W4301202222 doi "https://doi.org/10.1016/j.tca.2012.12.017" @default.
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