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• W4306844445 abstract "We explore the suitability of operando attenuated total reflection infrared (ATR-IR) spectroscopy methodologies for the study of organoaluminate electrolytes for Mg battery applications. The all-phenyl complex in tetrahydrofuran (THF), with the molecular structure [Mg2Cl3·6THF]+[AlPh4]-, is used as an exemplar electrolyte to compare two different spectroelectrochemical cell configurations. In one case, a Pt gauze is used as a working electrode, while in the second case, a thin (∼10 nm) Pt film working electrode is deposited directly on the surface of the ATR crystal. Spectroscopic measurements indicate substantial differences in the ATR-IR response for the two configurations, reflecting the different spatial arrangements of the working electrode with respect to the ATR sampling volume. The relative merits and potential pitfalls associated with the two approaches are discussed." @default.
• W4306844445 created "2022-10-20" @default.
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• W4306844445 date "2022-10-19" @default.
• W4306844445 modified "2023-10-14" @default.
• W4306844445 title "Methodologies for Operando ATR-IR Spectroscopy of Magnesium Battery Electrolytes" @default.
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• W4306844445 doi "https://doi.org/10.1021/acs.analchem.2c02843" @default.
• W4306844445 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36260706" @default.
• W4306844445 hasPublicationYear "2022" @default.
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