Matches in SemOpenAlex for { <https://semopenalex.org/work/W4307584732> ?p ?o ?g. }
- W4307584732 endingPage "2200668" @default.
- W4307584732 startingPage "2200668" @default.
- W4307584732 abstract "A nontarget screening method was developed based on D-optimal designs for ultra-high performance supercritical fluid chromatography with positive and negative electrospray ionization mode mass spectrometry. A mixture of organic contaminants such as pesticides, steroids, surfactants, phenolic and fatty acids, and polycyclic aromatic hydrocarbon derivatives, was used for the optimization. An aprotic mixture of dichloromethane and acetone [3:1] performed overall best as the injection solvent. The highest peak capacities (n) were accomplished at the shallowest gradient (1%B/min), ammonium formate (n = 378 in negative ionization mode), or ammonium acetate (n = 327 in positive ionization mode) in methanol as the modifier. Capillary voltage, make-up solvent flow rate, water, and additive concentration were the most significant factors for improving peak intensity: higher peak intensities were obtained at lower additive concentrations (5mM ammonium formate), and with 5% water in positive ionization mode. Conversely, water had detrimental effects in negative ionization mode. The optimized method was used to quantify organic contaminants in 17 freshwater sediment samples from Copenhagen, Denmark. Out of 50 monitored contaminants, 35 were detected in at least one sample. Further, the method has a potential for target and nontarget screening analysis of organic contaminants in solid matrices." @default.
- W4307584732 created "2022-11-03" @default.
- W4307584732 creator A5002354893 @default.
- W4307584732 creator A5028580773 @default.
- W4307584732 creator A5054582413 @default.
- W4307584732 date "2022-11-10" @default.
- W4307584732 modified "2023-09-27" @default.
- W4307584732 title "Ultra‐high‐performance supercritical fluid chromatography‐mass spectrometry for the analysis of organic contaminants in sediments" @default.
- W4307584732 cites W1971778241 @default.
- W4307584732 cites W1978216187 @default.
- W4307584732 cites W1987572231 @default.
- W4307584732 cites W1992301911 @default.
- W4307584732 cites W1995427895 @default.
- W4307584732 cites W2001349870 @default.
- W4307584732 cites W2008944014 @default.
- W4307584732 cites W2011238731 @default.
- W4307584732 cites W2021828609 @default.
- W4307584732 cites W2032685974 @default.
- W4307584732 cites W2048178510 @default.
- W4307584732 cites W2064247035 @default.
- W4307584732 cites W2064900248 @default.
- W4307584732 cites W2076545826 @default.
- W4307584732 cites W2081844255 @default.
- W4307584732 cites W2083637865 @default.
- W4307584732 cites W2232950086 @default.
- W4307584732 cites W2248036952 @default.
- W4307584732 cites W2335483232 @default.
- W4307584732 cites W2396142233 @default.
- W4307584732 cites W2412550358 @default.
- W4307584732 cites W2462175440 @default.
- W4307584732 cites W2592975068 @default.
- W4307584732 cites W2620711898 @default.
- W4307584732 cites W2725369953 @default.
- W4307584732 cites W2750303339 @default.
- W4307584732 cites W2763131723 @default.
- W4307584732 cites W2765677254 @default.
- W4307584732 cites W2798263195 @default.
- W4307584732 cites W2884991008 @default.
- W4307584732 cites W2904599458 @default.
- W4307584732 cites W2906313090 @default.
- W4307584732 cites W2906793873 @default.
- W4307584732 cites W2964237212 @default.
- W4307584732 cites W3028341635 @default.
- W4307584732 cites W3207941893 @default.
- W4307584732 cites W3208732044 @default.
- W4307584732 cites W4231559319 @default.
- W4307584732 cites W4307584732 @default.
- W4307584732 cites W774422765 @default.
- W4307584732 doi "https://doi.org/10.1002/jssc.202200668" @default.
- W4307584732 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36308040" @default.
- W4307584732 hasPublicationYear "2022" @default.
- W4307584732 type Work @default.
- W4307584732 citedByCount "2" @default.
- W4307584732 countsByYear W43075847322022 @default.
- W4307584732 countsByYear W43075847322023 @default.
- W4307584732 crossrefType "journal-article" @default.
- W4307584732 hasAuthorship W4307584732A5002354893 @default.
- W4307584732 hasAuthorship W4307584732A5028580773 @default.
- W4307584732 hasAuthorship W4307584732A5054582413 @default.
- W4307584732 hasBestOaLocation W43075847321 @default.
- W4307584732 hasConcept C107872376 @default.
- W4307584732 hasConcept C112570922 @default.
- W4307584732 hasConcept C118419359 @default.
- W4307584732 hasConcept C161790260 @default.
- W4307584732 hasConcept C162356407 @default.
- W4307584732 hasConcept C178790620 @default.
- W4307584732 hasConcept C179998833 @default.
- W4307584732 hasConcept C185592680 @default.
- W4307584732 hasConcept C18903297 @default.
- W4307584732 hasConcept C2775986502 @default.
- W4307584732 hasConcept C2780178953 @default.
- W4307584732 hasConcept C2780400988 @default.
- W4307584732 hasConcept C2780471494 @default.
- W4307584732 hasConcept C2780782300 @default.
- W4307584732 hasConcept C40684141 @default.
- W4307584732 hasConcept C43617362 @default.
- W4307584732 hasConcept C86803240 @default.
- W4307584732 hasConceptScore W4307584732C107872376 @default.
- W4307584732 hasConceptScore W4307584732C112570922 @default.
- W4307584732 hasConceptScore W4307584732C118419359 @default.
- W4307584732 hasConceptScore W4307584732C161790260 @default.
- W4307584732 hasConceptScore W4307584732C162356407 @default.
- W4307584732 hasConceptScore W4307584732C178790620 @default.
- W4307584732 hasConceptScore W4307584732C179998833 @default.
- W4307584732 hasConceptScore W4307584732C185592680 @default.
- W4307584732 hasConceptScore W4307584732C18903297 @default.
- W4307584732 hasConceptScore W4307584732C2775986502 @default.
- W4307584732 hasConceptScore W4307584732C2780178953 @default.
- W4307584732 hasConceptScore W4307584732C2780400988 @default.
- W4307584732 hasConceptScore W4307584732C2780471494 @default.
- W4307584732 hasConceptScore W4307584732C2780782300 @default.
- W4307584732 hasConceptScore W4307584732C40684141 @default.
- W4307584732 hasConceptScore W4307584732C43617362 @default.
- W4307584732 hasConceptScore W4307584732C86803240 @default.
- W4307584732 hasIssue "1" @default.
- W4307584732 hasLocation W43075847321 @default.
- W4307584732 hasLocation W43075847322 @default.
- W4307584732 hasLocation W43075847323 @default.