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• W4307899381 endingPage "170108" @default.
• W4307899381 startingPage "170108" @default.
• W4307899381 abstract "A sol–gel auto-combustion method is used in this study to synthesize a new class of single-phase high-entropy oxide (HEO) (Mg1/6Zn1/6Mn1/6Co1/6Ni1/6Fe1/6)3O4. The as-synthesized compound exhibits a single-phase spinel structure with an 8.3224 Å lattice parameter and an average crystallite size of 10 nm as determined by X-ray diffraction (XRD) data analysis. Raman and Fourier transform infrared results are in agreement with the XRD results. A scanning electron microscopy-based energy dispersed spectroscopy study suggests the formation of a porous structured morphology with a uniform elemental distribution. In addition, high-resolution transmission electron microscopy and surface analyses further confirm the formation of a pure spinel structure with a particle size of 12–20 nm and a mesoporous character with a pore size of 4.55 nm. X-ray photoelectron spectroscopy indicates mixed-valence states of elements (Mn, Fe, Co, and Ni) and their occupations over tetrahedral and octahedral sites. The temperature-dependent magnetization exhibited a bifurcation between zero-field-cooled and field-cooled magnetizations. From the M−H curves, the magnetization decreased monotonically with the increase in temperature (M is 22 emu/g at 2 K and 7.2 emu/g at 300 K). The coercivity decreased by approximately-one order of magnitude (HC = 1700 Oe at 2 K and HC = 200 Oe at 370 K). Finally, a comprehensive magnetic characterization of the as-synthesized HEO indicates their ferrimagnetic nature. The novel physical properties of the as-synthesized HEO could be useful in various potential applications." @default.
• W4307899381 created "2022-11-06" @default.
• W4307899381 creator A5025665745 @default.
• W4307899381 creator A5055371254 @default.
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• W4307899381 date "2022-12-01" @default.
• W4307899381 modified "2023-10-07" @default.
• W4307899381 title "Structure and magnetic properties of (Mg1/6Zn1/6Mn1/6Co1/6Ni1/6Fe1/6)3O4 nanocrystalline high-entropy oxide synthesized using a sol-gel auto combustion approach" @default.
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• W4307899381 doi "https://doi.org/10.1016/j.jmmm.2022.170108" @default.
• W4307899381 hasPublicationYear "2022" @default.
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