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• W4308141305 endingPage "116506" @default.
• W4308141305 startingPage "116506" @default.
• W4308141305 abstract "Reduction of spent nuclear fuel (SNF) components to metals during the electrolysis of the LiCl-Li 2 O melt at 650 °C is extremely important in the framework of the development of fuel reprocessing technology. In the present paper the ZrO 2 reduction by lithium during the electrolysis of the LiCl-Li 2 O melt at 650 °C was studied. Cathode processes on a molybdenum substrate in contact with different ZrO 2 samples (powder, pressed pellet, dense ceramic) were analyzed using cyclic voltammetry and electrolysis. It was shown that the appearance of ZrO 2 near the molybdenum cathode leads to increasing cathode currents and decreasing lithium oxidation current. Both effects indicate the consumption of reduced lithium for the reduction of ZrO 2 samples. In order to analyze the reduction products X-ray phase analysis and scanning electron microscopy were used, and to estimate the reduction degree of ZrO 2 samples three methods were tested: dissolution of samples in inorganic acid solution, dissolution of samples in EtOAc/Br 2 solution, and carbothermal reduction. It was shown that during the electrolysis of dense samples only the lithium zirconate (Li 2 ZrO 3 ) was formed at their surfaces, whereas the electrolysis of ZrO 2 powder samples resulted in the formation of Li 2 ZrO 3 , Zr 3 O, and ZrO phases." @default.
• W4308141305 created "2022-11-08" @default.
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• W4308141305 date "2022-11-01" @default.
• W4308141305 modified "2023-09-27" @default.
• W4308141305 title "Reduction of ZrO₂ in LiCl-Li₂O Melt During Electrolysis" @default.
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• W4308141305 doi "https://doi.org/10.1149/1945-7111/ac9f73" @default.
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