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• W4308190045 abstract "An efficient two-step procedure for the syntheses of pyrimidine nucleosides is presented. A series of glycosyl 5-(aminomethylene)-1,3-dioxane-4,6-dione derivatives were prepared from β-anomeric isonitriles by reaction with Meldrum’s acid or by allowing aminomethylene Meldrum’s acid to react with an 1-aldofuranosyl halide or acetate. The resultant 5-(aminomethylene)-1,3-dioxane-4,6-dione derivatives underwent reaction with benzyl- or 2,4-dimethoxybenzyl isocyanate via transacylation to provide uridine-5-carboxylic acid derivatives and related nucleosides. These nucleoside carboxylic acids were converted into other C-5 derivatives by bromo-decarboxylation with N-bromosuccinimide." @default.
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• W4308190045 date "2022-11-04" @default.
• W4308190045 modified "2023-09-27" @default.
• W4308190045 title "Pyrimidine Nucleosides Syntheses by Late-Stage Base Heterocyclization Reactions" @default.
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• W4308190045 doi "https://doi.org/10.1021/acs.orglett.2c03152" @default.
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