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• W4308678855 abstract "A metal-free radical 1,2-difunctionalization of activated alkenes with various silanes and tert-butyl nitrite is reported. The radical cascade occurs by light-promoted homolytic O–NO bond cleavage of tert-butyl nitrite and subsequent hydrogen atom abstraction by the alkoxyl radical from the silane. Silyl radical addition to the alkene and highly selective cross-coupling of the NO radical with the Si-adduct C-radical provide the silyl-oximation product in moderate to good yields. The reaction features good functional group tolerance and is easily scaled up." @default.
• W4308678855 created "2022-11-14" @default.
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• W4308678855 date "2022-11-10" @default.
• W4308678855 modified "2023-10-04" @default.
• W4308678855 title "Visible-Light-Mediated Radical Silyl-Oximation of Activated Alkenes Using <i>tert</i>-Butyl Nitrite and Silanes" @default.
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• W4308678855 doi "https://doi.org/10.1021/acs.orglett.2c03644" @default.
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