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- W4309112095 abstract "Abstract Nitroepoxides were introduced as efficient substrates for the one-pot three-component synthesis of 2-iminothiazoles under catalyst-free conditions. Reaction of amines, isothiocyanates, and nitroepoxides in THF at 10–15°C afforded corresponding 2-iminothiazoles in high to excellent yields. The reaction proceeds via the in situ formation of thiourea from an amine and an isothiocyanate, followed by nitroepoxide ring opening with the sulfur of thiourea, cyclization reaction, and dehydration cascade. The structures of products were confirmed by IR, NMR, HRMS analyses and X-ray crystallography." @default.
- W4309112095 created "2022-11-22" @default.
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- W4309112095 date "2022-11-15" @default.
- W4309112095 modified "2023-10-18" @default.
- W4309112095 title "Catalyst-free one-pot three-component synthesis of 2-iminothiazoles from nitroepoxides" @default.
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- W4309112095 doi "https://doi.org/10.21203/rs.3.rs-2252362/v1" @default.
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