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- W4309113359 endingPage "8050" @default.
- W4309113359 startingPage "8050" @default.
- W4309113359 abstract "Extrinsic chemiluminescence can be an efficient tool for determining pesticides and fungicides, which do not possess any intrinsic fluorescent signal. On this basis, (3-aminopropyl) trimethoxysilane (APTMS)-coated ZnO (APTMS@ZnO) was synthesized and tested as an extrinsic probe for the fungicide penconazole. Several synthetic routes were probed using either a one-pot or two-steps method, in order to ensure both a green synthetic pathway and a good signal variation for the penconazole concentration. The synthesized samples were characterized using X-ray diffraction (XRD), infrared (IR), Raman and ultraviolet-visible (UV-Vis) spectroscopy, scanning electron microscopy (SEM) imaging and associated energy-dispersive X-ray (EDX) analysis. The average size of the synthesized ZnO nanoparticles (NPs) is 54 ± 10 nm, in line with previous preparations. Of all the samples, those synthesized in two steps, at temperatures ranging from room temperature (RT) to a maximum of 40 °C, using water solvent (G-APTMG@ZnO), appeared to be composed of nanoparticles, homogeneously coated with APTMS. Chemiluminescence tests of G-APTMG@ZnO, in the penconazole concentration range 0.7–1.7 ppm resulted in a quenching of the native signal between 6% and 19% with a good linear response, thus indicating a green pathway for detecting the contaminant. The estimated detection limit (LOD) is 0.1 ± 0.01 ppm." @default.
- W4309113359 created "2022-11-22" @default.
- W4309113359 creator A5010796479 @default.
- W4309113359 creator A5010852355 @default.
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- W4309113359 creator A5021377848 @default.
- W4309113359 creator A5030446470 @default.
- W4309113359 creator A5050398976 @default.
- W4309113359 creator A5071832307 @default.
- W4309113359 date "2022-11-15" @default.
- W4309113359 modified "2023-09-26" @default.
- W4309113359 title "Syntheses of APTMS-Coated ZnO: An Investigation towards Penconazole Detection" @default.
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