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- W4309176372 abstract "The straightforward, continuous-flow synthesis of cyclopropyl carbaldehydes and ketones has been developed starting from 2-hydroxycyclobutanones and aryl thiols. This acid-catalyzed mediated procedure allows access to the multigram and easily scalable synthesis of cyclopropyl adducts under mild conditions, using reusable Amberlyst-35 as a catalyst. The resins, suitably ground and used for filling steel columns, have been characterized via TGA, ATR, SEM and BET analyses to describe the physical-chemical properties of the packed bed and the continuous-flow system in detail. To highlight the synthetic versatility of the arylthiocyclopropyl carbonyl compounds, a series of selective oxidation reactions have been performed to access sulfoxide and sulfone carbaldehyde cyclopropanes, oxiranes and carboxylic acid derivatives." @default.
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- W4309176372 date "2022-11-16" @default.
- W4309176372 modified "2023-10-14" @default.
- W4309176372 title "Continuous-Flow Synthesis of Arylthio-Cyclopropyl Carbonyl Compounds" @default.
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- W4309176372 doi "https://doi.org/10.3390/molecules27227943" @default.
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