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• W4309263617 abstract "The Dawson-type sulfate polyoxometalate (POM) [S2W18O62]4- has successfully been entrapped in polypyrrole (PPy) films on glassy carbon electrode (GCE) surfaces through pyrrole electropolymerization. Films of varying POM loadings (i.e., thickness) were grown by chronocoulometry. Film-coated electrodes were then characterized using voltammetry, revealing POM surface coverages ranging from 1.9 to 11.7 × 10-9 mol·cm-2, and were stable over 100 redox cycles. Typical film morphology and composition were revealed to be porous using atomic force microscopy, scanning electron microscopy, and X-ray photoelectron spectroscopy, and the effects of this porosity on POM redox activity were probed using AC impedance. The hybrid organic-inorganic films exhibited a good electrocatalytic response toward the reduction of iodate with a sensitivity of 0.769 μA·cm-2·μM-1." @default.
• W4309263617 created "2022-11-25" @default.
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• W4309263617 date "2022-11-17" @default.
• W4309263617 modified "2023-09-27" @default.
• W4309263617 title "Organic–Inorganic Hybrid Films of the Sulfate Dawson Polyoxometalate, [S₂W₁₈O₆₂]^4–, and Polypyrrole for Iodate Electrocatalysis" @default.
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• W4309263617 doi "https://doi.org/10.1021/acsomega.2c01287" @default.
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