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- W4309264972 abstract "The asymmetric hydrogenation of α-halogenated ketones with iridium catalyst was developed, utilizing easily accessed cinchona-alkaloid-based NNP ligands. Various α-chloroacetophenones, heterocyclic thienyl and furanyl substrates, and even bromoketones were completely converted to the desired chiral halohydrins by this protocol. Both (R)- and (S)-chiral halohydrins can be prepared by changing the configurations of the chiral ligand NNP with up to 99.6% ee (enantiomeric excess) and 98.8% ee, respectively. Also, a gram-scale experiment was carried out efficiently." @default.
- W4309264972 created "2022-11-25" @default.
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- W4309264972 date "2022-11-17" @default.
- W4309264972 modified "2023-10-15" @default.
- W4309264972 title "The Ir-Catalyzed Asymmetric Hydrogenation of α-Halogenated Ketones Utilizing Cinchona-Alkaloid-Derived NNP Ligand to Produce (<i>R</i>)- and (<i>S</i>)-Halohydrins" @default.
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- W4309264972 doi "https://doi.org/10.1021/acs.joc.2c02109" @default.
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