Matches in SemOpenAlex for { <https://semopenalex.org/work/W4309698079> ?p ?o ?g. }
Showing items 1 to 75 of
75
with 100 items per page.
- W4309698079 endingPage "124106" @default.
- W4309698079 startingPage "124106" @default.
- W4309698079 abstract "Using open tubular (OT) capillary columns in the nano and micro liquid chromatography scales has several advantages over conventional large-bore packed columns. Among the open tubular columns, those of the PLOT (porous layer open tubular) type are more suitable for liquid chromatography due to the porous character of the stationary phase that provides more significant interaction with the analytes. In addition, recent instrumental advances in capillaryLC coupled with mass spectrometry (MS) have opened up new avenues for developing and applying OT-LC-MS. This work discusses the possibility of applying PLOT columns in the capillary LC flow range (0.5–2 μL min −1 ) and describes the preparation, optimization, and evaluation of those columns. Poly(styrene-divinylbenzene) (PS-DVB) was used as the stationary phase, and the internal diameter of the columns discussed in this work was 10 and 25 μm. A comparison between these diameters is presented regarding fabrication and practical aspects of the operation. Additionally, for the 25 μm PLOT column, the gradient window and the flow rate effects on the system's performance were investigated. Flow rates of 1 μL min −1 and a gradient window of 60% (from 20 to 80% of acetonitrile) were the best conditions to work on this column in capillary LC conditions. • Preparation of Poly(styrene-divinylbenzene)Porous-Layer Open Tubular (PLOT) columns. • Application of PLOT columns at capillary scale flow rate. • Advantages and limitations of preparing and applying PLOT column." @default.
- W4309698079 created "2022-11-29" @default.
- W4309698079 creator A5012414720 @default.
- W4309698079 creator A5069601396 @default.
- W4309698079 creator A5087057938 @default.
- W4309698079 date "2023-02-01" @default.
- W4309698079 modified "2023-10-14" @default.
- W4309698079 title "Practical aspects of preparation, optimization, and evaluation of poly(styrene-divinylbenzene)porous-layer open tubular (PLOT) columns for capillary liquid chromatography" @default.
- W4309698079 cites W1988411294 @default.
- W4309698079 cites W1998347497 @default.
- W4309698079 cites W1999836467 @default.
- W4309698079 cites W2001446499 @default.
- W4309698079 cites W2065429223 @default.
- W4309698079 cites W2092858260 @default.
- W4309698079 cites W2126586165 @default.
- W4309698079 cites W2331457993 @default.
- W4309698079 cites W2523729262 @default.
- W4309698079 cites W2772682263 @default.
- W4309698079 cites W2927670091 @default.
- W4309698079 cites W2990237708 @default.
- W4309698079 cites W3129817992 @default.
- W4309698079 cites W3159847008 @default.
- W4309698079 doi "https://doi.org/10.1016/j.talanta.2022.124106" @default.
- W4309698079 hasPublicationYear "2023" @default.
- W4309698079 type Work @default.
- W4309698079 citedByCount "2" @default.
- W4309698079 countsByYear W43096980792023 @default.
- W4309698079 crossrefType "journal-article" @default.
- W4309698079 hasAuthorship W4309698079A5012414720 @default.
- W4309698079 hasAuthorship W4309698079A5069601396 @default.
- W4309698079 hasAuthorship W4309698079A5087057938 @default.
- W4309698079 hasConcept C15920480 @default.
- W4309698079 hasConcept C159985019 @default.
- W4309698079 hasConcept C178790620 @default.
- W4309698079 hasConcept C185592680 @default.
- W4309698079 hasConcept C192562407 @default.
- W4309698079 hasConcept C196806460 @default.
- W4309698079 hasConcept C2777566558 @default.
- W4309698079 hasConcept C2777682263 @default.
- W4309698079 hasConcept C43617362 @default.
- W4309698079 hasConcept C521977710 @default.
- W4309698079 hasConcept C6648577 @default.
- W4309698079 hasConceptScore W4309698079C15920480 @default.
- W4309698079 hasConceptScore W4309698079C159985019 @default.
- W4309698079 hasConceptScore W4309698079C178790620 @default.
- W4309698079 hasConceptScore W4309698079C185592680 @default.
- W4309698079 hasConceptScore W4309698079C192562407 @default.
- W4309698079 hasConceptScore W4309698079C196806460 @default.
- W4309698079 hasConceptScore W4309698079C2777566558 @default.
- W4309698079 hasConceptScore W4309698079C2777682263 @default.
- W4309698079 hasConceptScore W4309698079C43617362 @default.
- W4309698079 hasConceptScore W4309698079C521977710 @default.
- W4309698079 hasConceptScore W4309698079C6648577 @default.
- W4309698079 hasFunder F4320320997 @default.
- W4309698079 hasFunder F4320321091 @default.
- W4309698079 hasFunder F4320322025 @default.
- W4309698079 hasLocation W43096980791 @default.
- W4309698079 hasOpenAccess W4309698079 @default.
- W4309698079 hasPrimaryLocation W43096980791 @default.
- W4309698079 hasRelatedWork W1966915408 @default.
- W4309698079 hasRelatedWork W1993359912 @default.
- W4309698079 hasRelatedWork W2054374302 @default.
- W4309698079 hasRelatedWork W2075727959 @default.
- W4309698079 hasRelatedWork W2162964978 @default.
- W4309698079 hasRelatedWork W2349627637 @default.
- W4309698079 hasRelatedWork W2362205630 @default.
- W4309698079 hasRelatedWork W2365497346 @default.
- W4309698079 hasRelatedWork W2418694228 @default.
- W4309698079 hasRelatedWork W4239626584 @default.
- W4309698079 hasVolume "253" @default.
- W4309698079 isParatext "false" @default.
- W4309698079 isRetracted "false" @default.
- W4309698079 workType "article" @default.