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- W4309729042 abstract "The present work addresses, a development of novel analytical reagent 2, 4-dimethyl -3H-1, 5 benzodiazepine (DBA) for determination of rhodium (III) from a mixture of alloy, using extractive spectrophotometric technique. In this research, a novel analytical reagent has been explored and with NMR, IR and mass spectrometer techniques, its characterization was also reported. A reaction between Rhodium (III) and analytical reagent (DBA), resulted in to red-coloured compound, this red colored compound offers outstanding results at constant pH 8.9, when subjected to an extraction using n-butanol as selective solvent. The Beers law is fully satisfied in concentration range of 1 mg L-1 to 10 mg L-1 of rhodium (III) ions. The values of maximum absorption, average molar absorption co-efficient to the coloured compound were observed to be 510 nm, 4863L mol-1cm-2, however sandellâs sensitivity was recorded as 0.01205 μg cm-2. The determination of rhodium (III) metal traces from alloy mixture using DBA analytical reagent is revealed to be cheaper, effective and best than that of earlier spectrophotometric extraction methods." @default.
- W4309729042 created "2022-11-29" @default.
- W4309729042 creator A5034259829 @default.
- W4309729042 date "2022-11-22" @default.
- W4309729042 modified "2023-10-14" @default.
- W4309729042 title "Spectrophotometric Extraction method for Estimation of Rhodium (III) Using Novel Analytical Reagent" @default.
- W4309729042 doi "https://doi.org/10.12691/aees-10-11-4" @default.
- W4309729042 hasPublicationYear "2022" @default.
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