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- W4310259548 abstract "The main goal of research is to study ring-opening polymerization of L-lactide in the presence of multifunctional alcohols in order to determine the optimal conditions for synthesis of star-shaped molecules of a predetermined well-defined structure, which is necessary for fine adjustment of material properties for various biomedical applications. The degree of polymerization of 3-, 4- and 6-arm star-shaped poly(L-lactides) varied from 10 to 100 monomer units per arm. It was found that under the same conditions polymerization rate and rate of initiation of co-initiator's hydroxyl groups can vary significantly depending on the structure and concentration of the selected alcohol. To prove the absence of cyclic, linear and comet-like structures in synthesized star-shaped PLLA, a variety of instrumental methods were used including GPC with triple detection, 1H NMR and MALDI. Study of properties and supramolecular structure of poly(L-lactides) using DSC and WAXS demonstrated that branching limits segmental mobility of the PLLA chains, especially for short arms, and hinders crystallization of star-shaped poly(L-lactides)." @default.
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- W4310259548 date "2023-01-01" @default.
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- W4310259548 title "Synthesis and characterization of well-defined star-shaped poly(L-lactides)" @default.
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- W4310259548 doi "https://doi.org/10.1016/j.polymer.2022.125573" @default.
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