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• W4310336546 abstract "A transition-metal-free intramolecular redox cyclization reaction for the synthesis of cinnolines has been developed from 2-nitrobenzyl alcohol and benzylamine. Mechanistic investigations disclosed the involvement of a key intramolecular redox reaction, followed by condensation, azo isomerization to hydrazone, cyclization, and aromatization to form the desired products. Notably, the formation of intermediate 2-nitrosobenzaldehyde and (E)-2-(2-benzylidenehydrazineyl) benzaldehyde plays an important role in this transformation." @default.
• W4310336546 created "2022-12-08" @default.
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• W4310336546 date "2022-01-01" @default.
• W4310336546 modified "2023-09-26" @default.
• W4310336546 title "Intramolecular redox cyclization reaction access to cinnolines from 2-nitrobenzyl alcohol and benzylamine <i>via</i> intermediate 2-nitrosobenzaldehyde" @default.
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• W4310336546 doi "https://doi.org/10.1039/d2ra06523a" @default.
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