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• W4310421909 startingPage "16368" @default.
• W4310421909 abstract "The tetradentate azamacrocycle cyclam (=1,4,8,11-tetraazacyclotetradecane) was studied profoundly for the coordination of transition metal ions, and the resulting complexes were investigated extensively for their catalytic performance in, e.g., O2 activation and electrocatalytic CO2 reduction. Although the successful synthesis of analogous P4 macrocycles was described earlier, no tetradentate N,P mixed 14-membered macrocycles have been prepared to date and their chemistry remains elusive. Thus, in this work, we showcase the synthesis of phospha-aza mixed cyclam-based macrocycles by selectively exchanging one or two secondary amines in the macrocycle isocyclam (=1,4,7,11-tetraazacyclotetradecane) with tertiary phosphines. In addition, we herein present the preparation of the corresponding nickel complexes along with their complex chemical and structural characterization to provide first coordination studies." @default.
• W4310421909 created "2022-12-10" @default.
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• W4310421909 date "2022-11-30" @default.
• W4310421909 modified "2023-10-18" @default.
• W4310421909 title "Synthesis and Characterization of Phosphorus-Containing Isocyclam Macrocycles and Their Nickel Complexes" @default.
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• W4310421909 doi "https://doi.org/10.1021/acs.joc.2c02049" @default.
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