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• W4310943926 abstract "The development of a sustainable and simple catalytic system for N-formylation of N-heterocycles with methanol by direct coupling remains a challenge, owing to many competing side reactions, given the sensitivity of N-heterocycles to many catalytic oxidation or dehydrogenation systems. This work concerns the development of an in situ-generated CuI catalytic system for oxidative N-formylation of N-heterocycles with methanol that is based on the case study of a more typical 1,2,3,4-tetrahydroquinoline as substrate. Aside from N-heterocycles, some acyclic amines are also transformed into the corresponding N-formamides in moderate yields. Furthermore, a probable reaction mechanism and reaction pathway are proposed and extension of work based on some findings leads to a demonstration that the formed ⋅O2- and ⋅OOH radicals in the catalytic system is related to the formation of undesired tar-like products." @default.
• W4310943926 created "2022-12-21" @default.
• W4310943926 creator A5005360514 @default.
• W4310943926 creator A5005526774 @default.
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• W4310943926 creator A5057153132 @default.
• W4310943926 creator A5069623467 @default.
• W4310943926 creator A5081530707 @default.
• W4310943926 date "2023-01-02" @default.
• W4310943926 modified "2023-10-16" @default.
• W4310943926 title "In Situ‐Generated Cu^I Catalytic System for Oxidative <i>N</i>‐Formylation of N‐Heterocycles and Acyclic Amines with Methanol" @default.
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• W4310943926 doi "https://doi.org/10.1002/cssc.202202104" @default.

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