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- W4311544218 abstract "A novel and an efficient method for the synthesis of 3,5-bis(acyl)-1,2,4-thiadiazoles by the oxidative cyclization of α-oxothioamides with assistance of molecular iodine has been reported. The required substrates – α-oxothioamides have been synthesized by the reaction of α-oxodithioesters with ammonium chloride and sodium acetate. The probable mechanism for the formation of products has presented. A heterocyclization of two different α-oxothioamides furnished all four possible products. The protocol resulted in good to excellent yields under given conditions. Notably, reactions reported in this method can be used in scalable fashion." @default.
- W4311544218 created "2022-12-27" @default.
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- W4311544218 date "2023-02-01" @default.
- W4311544218 modified "2023-09-27" @default.
- W4311544218 title "Synthesis of 3,5-bis(acyl)-1,2,4-thiadiazoles via iodine mediated oxidative dimerization of α-oxothioamides" @default.
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- W4311544218 doi "https://doi.org/10.1016/j.tetlet.2022.154302" @default.
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