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• W4313252370 abstract "A FAU-X-rich porous monolith has been obtained by means of an unconventional two-stage method consisting of the production of a foamed geopolymeric precursor and its subsequent conversion by means of a hydrothermal method. The influence of the conversion process parameters, such as NaOH concentration (0.1–2 M), treatment temperature (40–80 °C) and time (24–72 h) on the FAU-X crystallization was studied. Collected data revealed that the highest yield in terms of zeolite content and FAU-X/LTA ratio was obtained performing the hydrothermal treatment with a 0.5 M NaOH solution at 60 °C. The crystallization kinetics of FAU-X inside the geopolymer precursor was investigated by means of Synchrotron Radiation X-Ray Diffraction Quantitative Phase Analysis (SR-XRD-QPA). Results showed that the crystallization starts after an induction time of about 3 days, and the weight percentage of the zeolite in the sample raises up to about 78% after 20 days of treatment. The highest yield in terms of zeolite content, about 80% of FAU-X and 6% of LTA, was reached at 20 days. Finally, Scanning Electron Microscopy (SEM) analysis showed the presence of well-defined octahedral crystals either on the pore surface or in the bulk of the sample starting from 3 days of hydrothermal treatment." @default.
• W4313252370 created "2023-01-06" @default.
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• W4313252370 date "2023-02-01" @default.
• W4313252370 modified "2023-09-25" @default.
• W4313252370 title "From geopolymers to zeolites: Synthesis and characterization of foamed FAU-X monoliths" @default.
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• W4313252370 doi "https://doi.org/10.1016/j.micromeso.2022.112426" @default.
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