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- W4313334528 abstract "An integrated strategy for the rapid and sensitive detection of deoxynivalenol in cereals was developed by combining Fe3O4 magnetic nanoparticle-modified metal organic framework-5-based magnetic solid-phase extraction and the optical fiber-based homogeneous chemiluminescence immunosensor. The hybrid magnetic material was prepared and characterized, exhibiting good enrichment capacity up to 1.68 mg/g. The competitive immunoassay-based homogeneous chemiluminescence immunosensor enabled washing-free and high-sensitivity detection of deoxynivalenol. Under optimized conditions, this immunosensor could detect deoxynivalenol as low as 46.7 pg/mL with a quantitatively linear range of 0.1 to 1000 ng/mL. The recoveries of this integrated detection strategy in rice, corn, and wheat ranged from 80.0 % to 118.2 %, 91.1 % to 116.7 %, and 80.0 % to 91.5 %, respectively, with a relative standard deviation that did not exceed 9.11 %. More importantly, it shows great consistency with the high-performance liquid chromatography-mass spectrometry in blind sample analysis. This integrated detection strategy provides a convenient approach for mycotoxins screening in cereals." @default.
- W4313334528 created "2023-01-06" @default.
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- W4313334528 date "2023-06-01" @default.
- W4313334528 modified "2023-09-29" @default.
- W4313334528 title "Rapid and quantitative determination of deoxynivalenol in cereal through the combination of magnetic solid-phase extraction and optical fiber-based homogeneous chemiluminescence immunosensor" @default.
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- W4313334528 doi "https://doi.org/10.1016/j.foodchem.2022.135356" @default.
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