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- W4313487923 abstract "High-pressure recrystallization could be the cheapest clean method of resolving enantiomers from the racemates defying Wallach's rule. We have investigated the effect of pressure on sodium tartrate monohydrate (NaTa·H2O), a notorious exception from Wallach's rule: both racemic polymorphs α-dl-NaTa·H2O and β-dl-NaTa·H2O are less dense than the enantiomers. According to the mobile-equilibrium principle, such high-density enantiomorphs should spontaneously separate under high pressures. The pressure dependence of the Gibbs free energy explains the preferential crystallization of mixed enantiomers of NaTa·H2O." @default.
- W4313487923 created "2023-01-06" @default.
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- W4313487923 date "2023-01-04" @default.
- W4313487923 modified "2023-09-23" @default.
- W4313487923 title "High-Pressure Crystallization and Thermodynamic Stability Study on the Resolution of High-Density Enantiomers from Low-Density Racemates" @default.
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- W4313487923 doi "https://doi.org/10.1021/acs.orglett.2c03747" @default.
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