Matches in SemOpenAlex for { <https://semopenalex.org/work/W4313571880> ?p ?o ?g. }
- W4313571880 endingPage "453" @default.
- W4313571880 startingPage "453" @default.
- W4313571880 abstract "In the course of the study, nanocrystalline cobalt monoboride was prepared by thermal decomposition of precursors [Co(DMF)6][An], where [An] = [B12H12]2− (1), [trans-B20H18]2− (2) or [B10Cl10]2− (3) in an argon atmosphere. Three new salt-like compounds 1–3 were prepared when Co(NO3)2 was allowed to react with (Et3NH)2[An]. Compound 1 is new; the structures of compounds 2 and 3 have been previously reported. Samples 1–3 were annealed at 900 °C in argon to form samples 1a–3a, which were characterized by single crystal XRD for 1 and powder XRD for 1–3. Powder XRD on the products showed the formation of BN and CoB for 1a in a 1:1 ratio; 2a gave a higher CoB:BN ratio but an overall decreased crystallinity. For 3a, only CoB was found. IR spectra of samples 1a–3a as well as X-ray spectral fluorescence analysis for 3a confirmed these results. The nanoparticular character of the decomposition products 1a–3a was shown using TEM; quite small particle sizes of about 10–15 nm and a quite normal size distribution were found for 1a and 2a, while the decomposition of 3 gave large particles with 200–350 nm and a broad distribution." @default.
- W4313571880 created "2023-01-06" @default.
- W4313571880 creator A5007483280 @default.
- W4313571880 creator A5017230585 @default.
- W4313571880 creator A5032131662 @default.
- W4313571880 creator A5046314129 @default.
- W4313571880 creator A5058226606 @default.
- W4313571880 creator A5066546560 @default.
- W4313571880 creator A5066621546 @default.
- W4313571880 creator A5073175818 @default.
- W4313571880 creator A5077121548 @default.
- W4313571880 creator A5088811740 @default.
- W4313571880 date "2023-01-03" @default.
- W4313571880 modified "2023-10-05" @default.
- W4313571880 title "A New Approach to the Synthesis of Nanocrystalline Cobalt Boride in the Course of the Thermal Decomposition of Cobalt Complexes [Co(DMF)6]2+ with Boron Cluster Anions" @default.
- W4313571880 cites W1969360633 @default.
- W4313571880 cites W1976419494 @default.
- W4313571880 cites W2034884777 @default.
- W4313571880 cites W2040634925 @default.
- W4313571880 cites W2043803752 @default.
- W4313571880 cites W2053051222 @default.
- W4313571880 cites W2053147630 @default.
- W4313571880 cites W2057575940 @default.
- W4313571880 cites W2059205366 @default.
- W4313571880 cites W2071429203 @default.
- W4313571880 cites W2073096489 @default.
- W4313571880 cites W2078275706 @default.
- W4313571880 cites W2083823674 @default.
- W4313571880 cites W2085990962 @default.
- W4313571880 cites W2101547779 @default.
- W4313571880 cites W2139047526 @default.
- W4313571880 cites W2227328155 @default.
- W4313571880 cites W2312468896 @default.
- W4313571880 cites W2330885755 @default.
- W4313571880 cites W2527848375 @default.
- W4313571880 cites W2604049092 @default.
- W4313571880 cites W2731097037 @default.
- W4313571880 cites W2739143282 @default.
- W4313571880 cites W2762421059 @default.
- W4313571880 cites W2794143300 @default.
- W4313571880 cites W2800732194 @default.
- W4313571880 cites W2883851309 @default.
- W4313571880 cites W2884456438 @default.
- W4313571880 cites W2967392452 @default.
- W4313571880 cites W2974028545 @default.
- W4313571880 cites W2985863612 @default.
- W4313571880 cites W2996403733 @default.
- W4313571880 cites W3011401501 @default.
- W4313571880 cites W3019590889 @default.
- W4313571880 cites W3048270404 @default.
- W4313571880 cites W3116524632 @default.
- W4313571880 cites W3127877102 @default.
- W4313571880 cites W3188719403 @default.
- W4313571880 cites W3198922294 @default.
- W4313571880 cites W4205351237 @default.
- W4313571880 cites W4220864010 @default.
- W4313571880 cites W4226050525 @default.
- W4313571880 cites W4283012193 @default.
- W4313571880 doi "https://doi.org/10.3390/molecules28010453" @default.
- W4313571880 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36615646" @default.
- W4313571880 hasPublicationYear "2023" @default.
- W4313571880 type Work @default.
- W4313571880 citedByCount "4" @default.
- W4313571880 countsByYear W43135718802023 @default.
- W4313571880 crossrefType "journal-article" @default.
- W4313571880 hasAuthorship W4313571880A5007483280 @default.
- W4313571880 hasAuthorship W4313571880A5017230585 @default.
- W4313571880 hasAuthorship W4313571880A5032131662 @default.
- W4313571880 hasAuthorship W4313571880A5046314129 @default.
- W4313571880 hasAuthorship W4313571880A5058226606 @default.
- W4313571880 hasAuthorship W4313571880A5066546560 @default.
- W4313571880 hasAuthorship W4313571880A5066621546 @default.
- W4313571880 hasAuthorship W4313571880A5073175818 @default.
- W4313571880 hasAuthorship W4313571880A5077121548 @default.
- W4313571880 hasAuthorship W4313571880A5088811740 @default.
- W4313571880 hasBestOaLocation W43135718801 @default.
- W4313571880 hasConcept C113196181 @default.
- W4313571880 hasConcept C124681953 @default.
- W4313571880 hasConcept C13965031 @default.
- W4313571880 hasConcept C140676511 @default.
- W4313571880 hasConcept C147789679 @default.
- W4313571880 hasConcept C160434732 @default.
- W4313571880 hasConcept C178790620 @default.
- W4313571880 hasConcept C179104552 @default.
- W4313571880 hasConcept C185592680 @default.
- W4313571880 hasConcept C187530423 @default.
- W4313571880 hasConcept C192562407 @default.
- W4313571880 hasConcept C46275449 @default.
- W4313571880 hasConcept C501308230 @default.
- W4313571880 hasConcept C515602321 @default.
- W4313571880 hasConcept C547737533 @default.
- W4313571880 hasConcept C8010536 @default.
- W4313571880 hasConceptScore W4313571880C113196181 @default.
- W4313571880 hasConceptScore W4313571880C124681953 @default.
- W4313571880 hasConceptScore W4313571880C13965031 @default.
- W4313571880 hasConceptScore W4313571880C140676511 @default.
- W4313571880 hasConceptScore W4313571880C147789679 @default.
- W4313571880 hasConceptScore W4313571880C160434732 @default.