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- W4313643060 abstract "During seven days, by keeping a colloidal solution of Au nanocrystals under solvent-saturated vapor pressure, two simultaneous 3D superlattices are produced. One grows at the air–liquid interface layer by layer (heterogenous growth), whereas the second one is formed in solution and precipitates. The remaining colloidal solution is still colored indicating the presence of nanocrystals. The building blocks of these two 3D superlattices are single-crystalline nanocrystals, whereas polycrystalline nanocrystals remain in suspension. The single-crystalline nanocrystals self-assemble into close-packed superlattices with long-range translational and orientational orderings, while polycrystalline nanocrystals behave like spheres with no preferential orientation. The face-to-face orientational ordering, which is only observed for single-crystalline nanocrystals, supports the relevance of the specific crystallinity-related morphologies of these nanocrystals in their better ability to self-assemble. Exploiting this spontaneous segregation would open up a simple alternative to other demanding routes for controlling crystallinity of nanocrystals and optimizing their properties. Single 3D superlattices with submillimeter size are built by self-assembly of Au nanocrystals with nearly similar size and different nanocrystallinities. The packing of such single 3D superlattices differs with the nanocrystallinity of their building blocks: with single-crystalline nanocrystals, the single 3D superlattices with orientation correlation within {110} colloidal crystal planes are characterized by the body-centered cubic (bcc) structures, whereas the 3D superlattice of polycrystalline building blocks is face-centered cubic (fcc) crystals." @default.
- W4313643060 created "2023-01-07" @default.
- W4313643060 date "2023-01-06" @default.
- W4313643060 modified "2023-10-02" @default.
- W4313643060 title "3 <scp>D</scp> Superlattice Growth in a Thermodynamic Equilibrium" @default.
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- W4313643060 doi "https://doi.org/10.1002/9783527344796.ch4" @default.
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