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- W4313647518 abstract "N,N'-Bis[2-(di-methyl-amino)-phen-yl]thio-urea, C17H22N4S (1), and N,N'-bis-[2-(di-ethyl-amino)-phen-yl]thio-urea, C21H30N4S (2), were prepared by the treatment of 1,1'-thio-carbonyl-diimidazole and 2 equivalents of 2-amino-N,N'-di-alkyl-aniline. Both compounds exhibit intra-molecular hydrogen bonds between the N-H(thio-urea) and NR2 (R = Me, Et) groups. The other N-H bonds face the sulfur atoms of S=C bonds in an adjacent mol-ecule, which forms an inter-molecular inter-action in the packed structure. The structural details match the spectroscopic data acquired from NMR and IR spectroscopy." @default.
- W4313647518 created "2023-01-07" @default.
- W4313647518 creator A5091445911 @default.
- W4313647518 date "2023-01-06" @default.
- W4313647518 modified "2023-09-30" @default.
- W4313647518 title "Synthesis, characterization, and crystal structures of <i>N</i>,<i>N</i>′-bis(2-dialkylaminophenyl)thioureas" @default.
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- W4313647518 doi "https://doi.org/10.1107/s2056989022012245" @default.
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