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- W4313893441 abstract "Nitrogen-doped carbon composites are prepared using simple precursors, such as glucose or urea and used as supports for Fe nanoparticles. The present work investigated two approaches for incorporating metal nanoparticles into the composite: traditional metal postloading and in situ formation of a metal/N-doped carbon catalyst. The impacts of the preparation technique on (i) the characteristics of the resulting iron oxides (Fe2O3 and Fe3O4) and (ii) the nanoparticle distribution on the support were determined. Microscopic surface characterization revealed that the postloading method promoted a uniform distribution of Fe nanoparticles (5–10 nm), which enhanced the activity and long-term stability of the catalytic system for the Baeyer–Villiger oxidation of cyclic ketones. The product yield reached 97% (5 h, 60 °C), and after the third reaction cycle, the yield remained at 96%. The proposed synthetic approach for preparing active and stable catalysts provides a new perspective for the inexpensive and sustainable synthesis of lactones." @default.
- W4313893441 created "2023-01-10" @default.
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- W4313893441 date "2023-02-01" @default.
- W4313893441 modified "2023-10-09" @default.
- W4313893441 title "Highly active and stable catalysts for Baeyer–Villiger oxidation – Traditional postloading vs in situ synthesis of Fe/N/C nanoparticles" @default.
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- W4313893441 doi "https://doi.org/10.1016/j.apcata.2023.119027" @default.
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