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- W4313909962 abstract "The synthesis and self-assembly of a high interaction parameter silicon-containing liquid crystalline block copolymer (Si-LCBCP) are reported, containing thermally and photo-responsive azobenzene mesogens in the side chains which undergo molecular structural transitions, influencing phase transitions and orientation in the block copolymer. A series of the azobenzene-containing Si-LCBCPs, poly{dimethylsiloxane-b-11-[4-(4-cyanophenylazo)phenoxy]undecane methacrylate}, were synthesized through atom transfer radical polymerization, and the bulk self-assembly as well as the influence of the liquid-crystalline (LC) phase transition of the LC block on the microphase-separated nanostructure of the BCPs is described. As the volume fraction of the PMAAzo block (fPMAAzo) changes from 41 to 71%, lamellar, double gyroid (GYR), orthorhombic Fddd network, hexagonally packed cylindrical (HEX), and body centered cubic nanostructures were obtained. When fPMAAzo = 55–57%, a thermally reversible HEX-GYR-Fddd phase transition induced by the temperature change and LC phase transition was observed. Bulk morphologies are compared with thin-film self-assembly, and pattern transfer into silica nanostructures is demonstrated." @default.
- W4313909962 created "2023-01-10" @default.
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- W4313909962 date "2023-01-10" @default.
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- W4313909962 title "Synthesis and Self-Assembly of Silicon-Containing Azobenzene Liquid Crystalline Block Copolymers" @default.
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- W4313909962 doi "https://doi.org/10.1021/acs.macromol.2c02343" @default.
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