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• W4316468550 endingPage "M1554" @default.
• W4316468550 startingPage "M1554" @default.
• W4316468550 abstract "5,5,7,7-Tetrametyl-6,7-dihydro-5H-dibenzo[c,e]azepine has been synthesized as a possible pro-chiral (or tropos) unit for the construction of a chiral catalyst and as a molecular chirality sensor for the absolute configuration assignment by chiroptical spectroscopy. A straightforward synthetic strategy for the preparation of the title compound in high overall yield through sequential addition of the four methyl groups on benzylic positions has been described. A VT-NMR study was used to determine the rotational barrier of the aryl–aryl bond in this biphenylazepine, revealing its torsional flexibility at room temperature, which makes the biphenylazepine suitable as both a chirality probe and a tropos moiety in chiral ligands." @default.
• W4316468550 created "2023-01-16" @default.
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• W4316468550 date "2023-01-16" @default.
• W4316468550 modified "2023-09-26" @default.
• W4316468550 title "5,5,7,7-Tetrametyl-6,7-dihydro-5H-dibenzo[c,e]azepine" @default.
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• W4316468550 doi "https://doi.org/10.3390/m1554" @default.
• W4316468550 hasPublicationYear "2023" @default.
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