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- W431673268 abstract "Ultra performance liquid chromatography tandem mass spectrometry (UPLC-MS/MS)method was successfully developed and validated for the analysis of simazine in fishand shrimp samples at trace levels to meet European Union requirements and importrequirements from certain countries. This method also utilized a simple, fast andinexpensive extraction technique called QuECheRS (quick, easy, cheap, rugged andsafe). Matrix-matched calibration standard are used to construct a calibration curve andEthoprophos is used as internal standard. At optimal conditions, the chromatographicseparation was achieved in less than 10 minutes with the total run time of 13.5 minutes.The mean recoveries for fish matrix ranged from 101 % to 107 % while shrimp matrixshows the range from 97 % to 101 %. Limit of detection (LOD) for simazine in fishand shrimp were 1.18 ng/g and 1.06 ng/g respectively. The limits of quantification(LOQ) were reported as 3.52 ng/g in fish matrix and 3.19 ng/g in shrimp matrix. Resultsfrom this study showed that the concentration of simazine obtained in fish and shrimpsamples were below the limit of quantification and it is reported as not detected in thesample." @default.
- W431673268 created "2016-06-24" @default.
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- W431673268 date "2014-01-01" @default.
- W431673268 modified "2023-09-27" @default.
- W431673268 title "Determination of simazine in fish and shrimp samples using ultra performance liquid chromatography tandem mass spectrometer (uplc-ms/ms) / Amirul Ashraf Bin Jamaluddin" @default.
- W431673268 hasPublicationYear "2014" @default.
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