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- W4319072726 abstract "Two new derivatives of 2,5-bis-cycloalkylsulfanyl-[1,3,4]thiadiazoles, i.e., 2,5-bis-cyclopentylsulfanyl-[1,3,4]thiadiazole and 2,5-bis-cyclohexylsulfanyl-[1,3,4]thiadiazole, were synthesized for a first time through a one-pot two-step procedure through the nucleophilic substitution of the potassium salt of 1,3,4-thiadiazole-2,5-dithiolate with chlorocyclopentane or bromocyclohexane in ethanol under reflux conditions. A cost-effective work-up was applied for the separation and purification of desired products. The products were characterized by physical and spectroscopic techniques. The long colorless needle-like crystals of 2,5-bis-cyclohexylsulfanyl-[1,3,4]thiadiazole were obtained, and its crystal structure was studied by single-crystal X-ray diffraction analysis. The transition phases and thermal stability of bismuthiol and two new bis-cycloalkyl bismuthiol were investigated by TGA/DTG and DSC. The thermal decomposition of bismuthiol was reported in the literature; herein, a detailed of its thermal behavior is analyzed for the first time. Finally, the biological activity of bismuthiol and two new bis-cyclopentylsulfanyl and bis-cyclohexylsulfanyl substituted bismuthiol derivatives were screened in vitro against the gram-negative (Escherichia coli ATCC 25922) and gram-positive (Staphylococcus aureus ATCC 25923) bacterial species by the disk diffusion method." @default.
- W4319072726 created "2023-02-04" @default.
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- W4319072726 date "2023-06-01" @default.
- W4319072726 modified "2023-09-27" @default.
- W4319072726 title "Synthesis and characterization of two new 2,5-bis-cycloalkylsulfanyl-[1,3,4]thiadiazoles and study of the crystal structure, thermal behavior, and biological activities compared with bismuthiol" @default.
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- W4319072726 doi "https://doi.org/10.1016/j.molstruc.2023.135087" @default.
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