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- W4319263720 abstract "Pentazolate compounds have attracted extensive attention as high energy density materials. The synthesis and recovery of pentazolate compounds is of great importance for their potential applications. Here, we report the synthesis of Pmn 2 1 -NaN 5 and Pm -Na 2 N 5 through compressing and laser heating pure NaN 3 at ∼ 60 GPa. Upon decompression, the pressure-induced structural transition from Pmn 2 1 -NaN 5 into Cm -NaN 5 is observed in the pressure range of 14–23 GPa for the first time. The cyclo- <?CDATA ${{rm{N}}}_{5}^{-}$?> <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML overflow=scroll> <mml:mrow> <mml:msubsup> <mml:mi mathvariant=normal>N</mml:mi> <mml:mn>5</mml:mn> <mml:mo>−</mml:mo> </mml:msubsup> </mml:mrow> </mml:math> can be traced down to 4.7 GPa at room temperature and recovered to ambient pressure under low temperature condition (up to 160 K). The Pm -Na 2 N 5 is suggested to decompose into the P 4/ mmm -NaN 2 at 23 GPa, and be stable at ambient conditions. This work provides insight into the high-pressure behaviors of pentazolate compounds and an alternative way to stabilize energetic polynitrogen compounds." @default.
- W4319263720 created "2023-02-06" @default.
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- W4319263720 date "2023-03-01" @default.
- W4319263720 modified "2023-09-28" @default.
- W4319263720 title "Pressure-induced structural transition and low-temperature recovery of sodium pentazolate" @default.
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- W4319263720 doi "https://doi.org/10.1088/1674-1056/acb917" @default.
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