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- W4319862092 abstract "[26394-89-8] C 9 H 19 N 2 O 2 SBr (MW 299.23) InChI = 1S/C9H19N2O2S.BrH/c1-6-13-8(12)7-14-9(10(2)3)11(4)5;/h6-7H2,1-5H3;1H/q+1;/p-1 InChIKey = YDNIXDGCACYVEJ-UHFFFAOYSA-M (odorless and stable, organic-soluble reagent used as a precursor for thiocarbonyl ylides, catalysts or as an activator for hydroxyl and carboxyl groups) 1 Physical Data: mp 130–131 °C. Solubility: soluble in most organic solvents. Form Supplied in: colorless solid. Preparative Methods: prepared by treatment of N,N,N,N -tetramethylthiourea ( TMTU ) with ethyl bromoacetate in EtOH [1 M] at 70 °C for 10 h. 1,2 Purification: evaporation of solvent under reduced pressure, followed by further drying under high vacuum. 1 Handling, Storage, and Precautions: reagent is bench stable." @default.
- W4319862092 created "2023-02-11" @default.
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- W4319862092 date "2023-01-13" @default.
- W4319862092 modified "2023-10-14" @default.
- W4319862092 title "2‐(2‐Ethoxy‐2‐oxoethyl)‐1,1,3,3‐tetramethylthiouronium bromide" @default.
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- W4319862092 doi "https://doi.org/10.1002/047084289x.rn02497" @default.
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