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- W4320482259 abstract "We explore the conversion of free-standing Cu nanowire arrays produced by electrodeposition in polymer etched ion-track membranes into metal-organic frameworks KHUST-1 by electrochemical oxidation. HKUST-1 particles are built up when the as-formed Cu 2+ ions bind to the benzene tricarboxylic acid ligands (BTC 3− ) in the electrolyte solution. The morphology and crystallinity of the samples at different transformation stages are investigated by scanning and transmission electron microscopy. X-ray diffraction data taken at different conversion times confirm the formation of HKUST-1 particles. The conversion process resulted in octahedral structures of several μ m in size. Comparison of the Raman spectra with the band positions derived from density functional theory (DFT) calculations, suggests that vibrations involving Cu atoms appear only below 490 cm −1 wavenumbers and involve the entire HKUST-1 lattice rather than vibrations of single bonds." @default.
- W4320482259 created "2023-02-14" @default.
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- W4320482259 date "2023-02-01" @default.
- W4320482259 modified "2023-10-18" @default.
- W4320482259 title "Electrochemical Conversion of Cu Nanowire Arrays into Metal-Organic Frameworks HKUST-1" @default.
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- W4320482259 doi "https://doi.org/10.1149/1945-7111/acbba4" @default.
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