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- W4321782773 abstract "Here we prepared a highly efficient and reusable catalyst by a step-by-step postsynthesis modification of UiO-66-NH2 metal–organic frameworks (MOFs) with nitrogen-rich organic ligands and used it as support for the preparation of UiO-66-NH2@cyanuric chloride@2-aminopyrimidine/PdNPs. The catalytic performance’s results of UiO-66-NH2@cyanuric chloride@2-aminopyrimidine/PdNPs, UiO-66-NH2/PdNPs, and UiO-66-NH2@cyanuric chloride/PdNPs indicate high efficiency of the modulation of the microenvironment of the palladium NPs. The addition of N-rich organic ligands through postsynthesis modification caused a unique structure of the final composite in favor of the progress of the C–C coupling reaction. Various techniques, including FT-IR, XRD, SEM, TEM, EDS, and elemental mapping, were used to characterize UiO-66-NH2@cyanuric chloride@2-aminopyrimidine/PdNPs, indicating its successful preparation. Three C–C coupling reactions, including the Suzuki, Heck, and Sonogashira coupling reactions, were promoted using the produced catalyst. As a result of the postsynthesis modification (PSM), the proposed catalyst displays improved catalytic performance. In addition, the suggested catalyst was highly recyclable up to ten times without leaching of PdNPs." @default.
- W4321782773 created "2023-02-25" @default.
- W4321782773 creator A5016572296 @default.
- W4321782773 creator A5080856581 @default.
- W4321782773 creator A5090025959 @default.
- W4321782773 date "2023-02-24" @default.
- W4321782773 modified "2023-10-13" @default.
- W4321782773 title "Stabilization of Palladium-Nanoparticle-Decorated Postsynthesis-Modified Zr-UiO-66 MOF as a Reusable Heterogeneous Catalyst in C–C Coupling Reaction" @default.
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- W4321782773 doi "https://doi.org/10.1021/acsomega.2c07661" @default.
- W4321782773 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36910943" @default.
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