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• W4321792101 abstract "Abstract The Li x FePO 4 cathode material with x = 1.00, 1.05, 1.10, 1.15, and 1.20 has been synthesized by chemical precipitation method. The particles of Li x FePO 4 material are further in‐situ coated with emeraldine salt (ES) polymer. These ES coated Li x FePO 4 (Li x FePO 4 ‐ES) particles have been characterized by XRD, FE‐SEM, TEM, and DTA/TG analyses. The XRD analysis of Li x FePO 4 indicates the formation of pure single phase of LiFePO 4 (for x = 1.00, 1.05, and 1.10). Excess of lithium have no influence on the crystal structure of Li x FePO 4 upto x = 1.10 and no other phase containing Li + is formed. The material Li x FePO 4 (for x = 1.15) shows low intensity peaks corresponding to Li 3 PO 4 phase at 2θ = 22.31° and 23.19°. The peaks are found significant for the composite material for x = 1.20. The micrograph of composite powder Li x FePO 4 ‐ES shows good coverage of Li x FePO 4 particle by PANI. The materials Li x FePO 4 and Li x FePO 4 ‐ES (x = 1.00–1.20) are tested for discharge capacity and electrochemical impedance measurements for cathode materials. The electrochemical impedance spectra of Li x FePO 4 ‐ES (x = 1.00 to 1.20) show low charge transfer resistance ( R ct ), as compared to Li x FePO 4 indicating polyaniline incorporation have offered good conductivity. The highest discharge capacity of 131 mAh g –1 is obtained at the current rate of 2C for Li x FePO 4 ‐ES (x = 1.10) cathode. The impurity phase that appears in the XRD pattern reduces the discharge capacity of Li x FePO 4 ‐ES (x = 1.15 and 1.20)." @default.
• W4321792101 created "2023-02-25" @default.
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• W4321792101 date "2023-02-01" @default.
• W4321792101 modified "2023-10-16" @default.
• W4321792101 title "Electrochemical Behavior of Emeraldine Salt Polymer Coated Li _x FePO ₄ Cathode Materials with Excess Lithium Doping" @default.
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• W4321792101 doi "https://doi.org/10.1002/masy.202100496" @default.
• W4321792101 hasPublicationYear "2023" @default.
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