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- W4323665469 abstract "The control of morphology, structure and composition of metal–organic frameworks derived metal-nitrogen doped porous carbon (M–N–C) with high precision and accuracy is essential for the catalytic performance. While single-atom or small-sized nanometer catalysts show notable effects in catalysis, one catalyst combining the advantages of single-atom and nanometer catalysts may cultivate more benefits. Herein, we designed and successfully fabricated a series of Fe-doped ZIF–x with different morphologies (cube→truncated hexahedron→truncated octahedron) in one pot by simply adjusting the adding amount of vitamin C. After high-temperature calcination, Fe3C integrated with Fe single-atom planted in N-doped carbon (FeSA/FeNC–N–C–x) with various morphology, structure and composition could be acquired. Among them, FeSA/FeNC–N–C–0.75 exhibited the best catalytic performance for the transfer hydrogenation of halogenated nitrobenzenes with N2H4·H2O under room temperature. Acid-leaching tests, poisoning experiments, and the density functional theory calculations showed that Fe3C integrated with Fe single-atom had a better catalytic effect than the separated Fe3C or Fe single-atom." @default.
- W4323665469 created "2023-03-10" @default.
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- W4323665469 date "2023-06-01" @default.
- W4323665469 modified "2023-10-16" @default.
- W4323665469 title "Fe3C nanoclusters integrated with Fe single-atom planted in nitrogen doped carbon derived from truncated hexahedron zeolitic imidazolate framework for the efficient transfer hydrogenation of halogenated nitrobenzenes" @default.
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- W4323665469 doi "https://doi.org/10.1016/j.jcis.2023.03.006" @default.
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