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- W4324069635 endingPage "108622" @default.
- W4324069635 startingPage "108622" @default.
- W4324069635 abstract "A new microextraction method as a facile, efficient, and safe intermediate sample preparation procedure was developed for simultaneous extraction and preconcentration of nickel (II), cobalt (II), and lead (II) in some vegetables and water samples. The new method uses a novel deep eutectic solvent as an extractant on the surface of a meltblown layer of a facemask with an iron wire inside of it. 2-(5-Bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP) was used as a chelating reagent. The concentrations of the enriched ions were measured using a flame atomic absorption spectrophotometer (FAAS). The introduced method underwent significant parameter optimization, which may influence the extraction process efficiency. Under the best situations, the calibration curve of the method showed excellent linearity over the concentration range 2–150 μg L−1, 3–150 μg L−1, and 7–500 μg L−1 have satisfactory coefficients of determination (R2 ≥ 0.998) for nickel (II), cobalt (II), and lead (II), respectively. Detection limits were within 0.61 – 2.30 μg L−1, and the relative standard deviation values were fewer than 2.6 % (n = 10). Experimental results indicated that the presented method has a high ability to cleanly and enrich metal ions in several samples, including natural water, dill, coriander, and spinach leaves, with limited solvent consumption and low operating costs." @default.
- W4324069635 created "2023-03-14" @default.
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- W4324069635 date "2023-07-01" @default.
- W4324069635 modified "2023-09-25" @default.
- W4324069635 title "Simultaneous preconcentration and determination of trace metals in edible plants and water samples by a novel solvent bar microextraction using a meltblown layer of facemask as the extractant phase holder combined with FAAS" @default.
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- W4324069635 doi "https://doi.org/10.1016/j.microc.2023.108622" @default.
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