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- W4327715432 abstract "Abstract We report a protocol for the synthesis of new dialkyl(1‐(organolthio)naphthalen‐2‐yl)phosphates and derivatives via a dehydrogenative phosphorylation reaction between functionalized naphthols and H ‐phosphonates. Diphenyl ditelluride was employed as an organocatalyst and sonochemistry as an alternative energy source. The reaction conditions were defined through a factorial design approach, and the best condition provided the synthesis of dialkyl(1‐(organolthio)naphthalen‐2‐yl)phosphates in yields that varied from 51–98 % under ultrasound irradiation after 2 h of sonication. The synthetic protocol was also effective for phenol and thiophenol starting materials. All products were characterized by state‐of‐the‐art spectroscopic and spectrometric techniques." @default.
- W4327715432 created "2023-03-18" @default.
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- W4327715432 date "2023-03-16" @default.
- W4327715432 modified "2023-10-02" @default.
- W4327715432 title "Synthesis of Phosphate Esters by Using Diphenyl Ditelluride as Organocatalyst" @default.
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- W4327715432 doi "https://doi.org/10.1002/ejoc.202300021" @default.
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