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• W4328007491 abstract "For obtaining microscopic knowledge toward a fabrication process of (Bi,Pb) <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> Sr <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> Ca <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> Cu <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>3</sub> O <italic xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>_x</i> (Bi,Pb-2223) single-phase material, we fabricated a multilayered film on a SrTiO <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>3</sub> (001) substrate by a sputtering method using (Bi,Pb) <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> Sr <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> CaCu <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>2</sub> O <italic xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>_y</i> (Bi,Pb-2212) and Pb–Ca–Cu–O targets alternately at 650 °C. The as-grown film was an epitaxially grown multilayered film consisting of Bi,Pb-2212 and Pb–Ca–Cu–O layers. Coarse grains of impurity phases were also formed within the multilayered film, and these impurity phases were difficult to eliminate even after heat treatments. After 10 h heat treatment at 840 °C with Bi,Pb-2223 pellets, the phase transition from Bi,Pb-2212 to Bi,Pb-2223 occurred in the multilayered film. The phase transition to Bi,Pb-2223 proceeded preferentially at the interface with the impurity phases and the Pb–Ca–Cu–O layers. These observation results suggest that the impurity phases promote three-dimensional atomic diffusion in the multilayered film to accelerate the phase transition to Bi,Pb-2223, as well as consume constituent elements, Ca, Cu and O. Even after the 100 h heat treatment at 840 °C with Bi,Pb-2223 pellets, the phase transition from Bi,Pb-2212 to Bi,Pb-2223 did not proceed completely, and the fraction of the Bi,Pb-2223 phase in the whole superconducting phases was ∼50%. It is suggested that controlling the formation and microstructure of the impurity phases is a key to further increasing the fraction of the Bi,Pb-2223 phase." @default.
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• W4328007491 date "2023-08-01" @default.
• W4328007491 modified "2023-09-25" @default.
• W4328007491 title "Microstructure and Its Heat Treatment Process of Thin Films Fabricated by Alternate Sputtering of (Bi,Pb)₂Sr₂CaCu₂O<i> _x </i> and Pb–Ca–Cu–O Targets on SrTiO₃ Substrates" @default.
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• W4328007491 doi "https://doi.org/10.1109/tasc.2023.3259920" @default.
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