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• W4328105765 endingPage "121593" @default.
• W4328105765 startingPage "121593" @default.
• W4328105765 abstract "Polycrystalline zeolitic-imidazolate framework-8 (ZIF-8) membranes have shown very promising for propylene/propane (C3) separation. Though high-performance ZIF-8 membranes have been prepared by various synthesis methods, secondary growth method offers unique advantages due to its decoupling of a seeding step and a growth step, leading to membranes with better microstructures, thereby not only better separation performances but also higher reproducibility. However, there are only a few reports on ZIF-8 membranes with ultra-high C3 separation factors (i.e., >200) that are made by secondary growth method. Here, we report polycrystalline ZIF-8 membranes by a secondary growth method modified with an addition of 1,4-butanediol (Bdiol). The membranes showed significantly improved C3 separation factors up to ∼283 as compared to those prepared without modification. It was found that adding Bdiol in the secondary growth solution improved the microstructures of the ZIF-8 membranes, thereby enhancing their C3 separation performances. Furthermore, the presence of Bdiol in the growth solution enabled formation of well-intergrown ZIF-8 membranes even with a low linker-to-metal ratio (∼16), otherwise not possible to form ZIF-8 membranes. Interestingly, the resulting membranes showed a plate-like morphology with the highest separation factor of ∼283 among those prepared. All membranes in this work exhibited enhanced C3 separation performances as compared to those synthesized without modification." @default.
• W4328105765 created "2023-03-22" @default.
• W4328105765 creator A5022700426 @default.
• W4328105765 creator A5060892538 @default.
• W4328105765 date "2023-07-01" @default.
• W4328105765 modified "2023-10-01" @default.
• W4328105765 title "Enhancing the C3 separation performances of polycrystalline ZIF-8 membranes by additive-assisted secondary growth" @default.
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• W4328105765 doi "https://doi.org/10.1016/j.memsci.2023.121593" @default.
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