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- W433653607 abstract "Inulin is a natural storage carbohydrate composed of a chain of fructose units with generally a terminal glucose unit, industnally extracted from chicory root and commercially available m the powdered form. In a previous study, we engineered physical properties and controlied the amorphous/crystallmity content of inulin by selecting appropriate feed temperature and/or mlet air temperature of the spray-drier. Unhke a crystalhne structure, the amorphous solid is metastable. Amorphous solids are commonly formed through rapid cooling of a liquid melt to a certain temperature so that the molecules m the melt do not hâve enough time to rearrange and are frozen in their original position. An amorphous solid is also called a glass, and is characterized by a glass transition, which refers to the phase transition when a glass is changed into a supercooled melt. The glass transition is an important parameter for understanding the mechamsms of transformation processes in foods and for controlling their shelf-Hfe. Depending on the moisture and/or the storage temperature, the amorphous product can physically change in order to attain a more thermo-dynamical stable state. For this reason, the aim of this work was to determine the kinetic of the physical changes of amorphous inulin powder stored at high relative humidity. The physical parameters investigated were the glass transition temperature (Tg) and the crystallinity index, determined by Modulated Differential Scanning Calorimetry (MDSC) and Wide Angle X-ray Scattering (WAXS), respectively. Temperature-resolved WAXS was used to understand the MDSC thermograms when crystallization occurred. In addition, surface analysis was used to correlate the measured parameters to the observed macroscopic property changes of the amorphous powder." @default.
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- W433653607 date "2008-07-01" @default.
- W433653607 modified "2023-09-27" @default.
- W433653607 title "Study of the stability and the physical property changes of amorphous inulin during moisture adsorption" @default.
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