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- W4360609148 abstract "An unprecedented electrochemical cross-dehydrogenative coupling reaction between isochroman and unactivated ketones to directly synthesize α-substituted isochromans has been developed. This strategy provides a facile and efficient procedure to the direct activation of C(sp3)-H bond adjacent to the O atom of isochroman. The method features high atom economy, chemical oxidant-free, and mild conditions, in which methanesulfonic acid (MsOH) acts as both electrolyte and catalyst, making the process more convenient and environmentally friendly. Gram-scale experiment and synthesis of antitumor active compounds demonstrate the great potential of this protocol for practical applications." @default.
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- W4360609148 date "2023-03-23" @default.
- W4360609148 modified "2023-10-05" @default.
- W4360609148 title "Electrochemical Cross-Dehydrogenative Coupling of Isochroman and Unactivated Ketones" @default.
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- W4360609148 doi "https://doi.org/10.1021/acs.joc.2c02616" @default.
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