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- W4360841890 abstract "A facile and novel strategy has been developed for synthesis of 24-(R)-hydroxycholesterol, a key intermediate of tacalcitol, starting from 24-dehydrocholesterol in seven steps with 48.2% overall yield and high diastereomer ratio. Photocatalytic oxidation of olefins by employing inexpensive Rose Bengal as photosensitizer and air as the sole oxidant for the preparation of Δ5,25-3β-Hydroxycholestadiene-24-one-3-acetate is the key step in this synthetic route. This developed strategy features mild conditions, satisfied total yield and excellent stereoselectivity (24-R/S = 97.7:2.3), providing a novel access to the 24-(R)-hydroxycholesterol." @default.
- W4360841890 created "2023-03-25" @default.
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- W4360841890 date "2023-07-01" @default.
- W4360841890 modified "2023-10-18" @default.
- W4360841890 title "Investigation on the synthesis of 24-(R)-hydroxycholesterol" @default.
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- W4360841890 doi "https://doi.org/10.1016/j.steroids.2023.109227" @default.
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