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- W4362637357 abstract "The nanoparticles of glycidoxy propyl POSS (GPOSS) and alumina microparticles were added into a two-part epoxy adhesive. The filler dispersion in adhesive samples were characterized by EDXA and SEM micrographs indicating weaker dispersion for the highly loaded alumina and/or GPOSS filled compositions. Comparing with neat epoxy resin, DSC thermograms revealed lower heat of cure and higher onset cure temperatures in all compositions. The highest glass transition temperature (Tg) was obtained for the composition containing 10 wt% alumina microparticles and 20 wt% GPOSS, which was about 44 °C higher than that of the neat epoxy. The thermal stability of this composition was improved up to 7 °C based on the first decomposition peak temperature in a TGA test. However, the highest char yield obtained from the TGA test was recorded for a composition containing 20 wt% alumina microparticles and 10 wt% GPOSS. Adhesive lap shear strength values showed a maximum of 13.2 MPa (>40% than epoxy) for the composition containing 10 wt% alumina microparticles and 10 wt% GPOSS. The improvement in adhesive thermal stability was further verified by the results of adhesive strength retention after heat aging at 200 °C for 24 h. It can be concluded that the simultaneous incorporation of GPOSS and alumina in an epoxy results in noticeable improvements in Tg, thermal stability and adhesion strength, mainly due to improved interfacial interactions between GPOSS and alumina particles." @default.
- W4362637357 created "2023-04-07" @default.
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- W4362637357 date "2023-05-01" @default.
- W4362637357 modified "2023-09-24" @default.
- W4362637357 title "A study of the thermal properties of alumina/glycidoxy propyl POSS/epoxy adhesives" @default.
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- W4362637357 doi "https://doi.org/10.1016/j.ijadhadh.2023.103368" @default.
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