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• W4362660796 abstract "While some promising materials for all-solid-state batteries are already extensively investigated in a lab scale, the transferability to mass production is still a limiting factor. β-lithium thiophosphate (β-Li3PS4) has good ionic conductivity and can be synthesized wet-chemically, which opens up the possibility for scale-up. For safe upscaling, the enthalpies of the synthesis steps need to be examined in order to handle exothermic and endothermic processes. Here, the reaction enthalpies of the wet-chemical synthesis of β-Li3PS4 in tetrahydrofuran (THF) are determined. The synthesis routine is established in a lab scale, and the synthesis success is confirmed via X-ray diffraction (XRD) and electrochemical impedance spectroscopy (EIS). The reaction of the educts in THF is investigated using a reaction calorimeter and shows a strongly exothermic process. The subsequent processes are examined using differential scanning calorimetry with thermogravimetric analysis and show a strong endothermic process during solvent removal and a slightly exothermic process during crystallization." @default.
• W4362660796 created "2023-04-07" @default.
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• W4362660796 date "2023-04-06" @default.
• W4362660796 modified "2023-10-01" @default.
• W4362660796 title "Determination of Reaction Enthalpies of Synthesizing β-Li₃PS₄ in Tetrahydrofuran" @default.
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• W4362660796 doi "https://doi.org/10.1021/acsomega.3c00603" @default.
• W4362660796 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37091412" @default.
• W4362660796 hasPublicationYear "2023" @default.
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