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- W4362721724 abstract "A novel electrochemical sensing platform based on composite material was prepared, consisting of molecularly imprinted polymer coated on graphene oxide (MIP-GO), for the selective and sensitive analysis of amoxicillin (AMOX). Amoxicillin (AMOX) is a newer version of penicillin which belongs to the β-lactam family. The monitoring of AMOX in food as well as in environment plays a crucial role in public health protection. Through Hummer's method, GO was prepared from graphite powder which was modified into its acid derivative by treating with 4-amino benzoic acid. It further undergoes surface modification with allyl bromide to form vinylated GO-O-CH2-CH=CH2. The polymerization process was carried out using methacrylic acid (MAA) as the monomer and ethylene glycol (EGDMA) as cross-linker, azobisisobutyronitrile (AIBN) as the initiator and AMOX as template molecule. The different preparatory stages of materials were characterized by using Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffractometer (XRD), and Scanning Electron Microscope (SEM). The detection limit of the present work is 10−10 M shows that prepared material is suitable for the detection of AMOX in deca-level concentrations. In addition to that GO-MIP based sensors exhibit excellent electrocatalytic performance in linear to the concentrations of AMOX with high selectivity in comparison with several other methods and it shows linearity from 10−7 to 10−10 M concentrations. Interference study was carried out using 1.0 µM solution of cephalexin, ampicillin and cloxacillin as well as AMOX. The optimum pH for the sensing of AMOX is pH 8.0 and GO-MIP sensor shows a good result, is due to the momentous sensitizing effect of material and increases electron transfer and surface area for big loading of GO-MIP" @default.
- W4362721724 created "2023-04-09" @default.
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- W4362721724 date "2023-08-01" @default.
- W4362721724 modified "2023-10-18" @default.
- W4362721724 title "Synthesis and characterization of modified graphene oxide based molecularly imprinted polymer for the detection of amoxicillin" @default.
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- W4362721724 doi "https://doi.org/10.1016/j.molstruc.2023.135528" @default.
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